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Synthesis and characterization the intercalation compound of SnS 2-ethylenediamine by hydrothermal reaction

  • Qing Lv*
  • , Caixia Li
  • , Danyu Jiang
  • , Qiang Li
  • *此作品的通讯作者
  • East China Normal University
  • CAS - Shanghai Institute of Ceramics

科研成果: 书/报告/会议事项章节会议稿件同行评审

摘要

The intercalation of ethylenediamine (en) into SnS2 was synthesised by hydrothermal reaction at the temperature of 180°C. And then dispersed the intercalation compounds in N, N-dimethylformamide (DMF) by stirring 48h, getting a light yellow sol, with the nature of uniform, transparent and stable. Analysised the structural of the product by means of X-ray powder diffraction (XRD). The morphology of sol was characterized by using of transmission electron microscopy (TEM). The UV-Vis spectrophotometer was utilized for the absorbance of the colloidal. The results show that en has been successfully inserted into the layer of tin disulphide, and the target products is of high purity and good crystal. The sol is of high stability and homogeneity, and have the strongest absorption at the Wavelength of 270nm.

源语言英语
主期刊名High-Performance Ceramics VII
出版商Trans Tech Publications Ltd
215-218
页数4
ISBN(印刷版)9783037854259
DOI
出版状态已出版 - 2012
活动7th China International Conference on High-Performance Ceramics, CICC-7 - Xiamen, 中国
期限: 4 11月 20117 11月 2011

出版系列

姓名Key Engineering Materials
512-515
ISSN(印刷版)1013-9826
ISSN(电子版)1662-9795

会议

会议7th China International Conference on High-Performance Ceramics, CICC-7
国家/地区中国
Xiamen
时期4/11/117/11/11

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