Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

Cai Hua Liu; Wen Juan Wang; Wen Ping Cheng; Xin Yu Yu; Jian Guo Yang; Ming Yuan He

doi:10.3724/SP.J.1077.2008.00171

Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

Cai Hua Liu^*
, Wen Juan Wang
, Wen Ping Cheng
, Xin Yu Yu
, Jian Guo Yang
, Ming Yuan He

^*此作品的通讯作者

化学与分子工程学院

East China Normal University

科研成果: 期刊稿件 › 文章 › 同行评审

5 引用（Scopus）

摘要

Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C₁₆mim]⁺Br^-) as template at room temperature and characterized by X-ray diffraction, N₂ adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

源语言	英语
页（从-至）	171-174
页数	4
期刊	Wuji Cailiao Xuebao/Journal of Inorganic Materials
卷	23
期	1
DOI	https://doi.org/10.3724/SP.J.1077.2008.00171
出版状态	已出版 - 1月 2008

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10.3724/SP.J.1077.2008.00171

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@article{71f02451f9394291ba0cca183cbbfd8a,

title = "Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41",

abstract = "Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.",

keywords = "Fe-MCM-41, Ionic liquid, Mesoporous molecular sieves",

author = "Liu, \{Cai Hua\} and Wang, \{Wen Juan\} and Cheng, \{Wen Ping\} and Yu, \{Xin Yu\} and Yang, \{Jian Guo\} and He, \{Ming Yuan\}",

year = "2008",

month = jan,

doi = "10.3724/SP.J.1077.2008.00171",

language = "英语",

volume = "23",

pages = "171--174",

journal = "Wuji Cailiao Xuebao/Journal of Inorganic Materials",

issn = "1000-324X",

publisher = "Science Press ",

number = "1",

}

TY - JOUR

T1 - Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

AU - Liu, Cai Hua

AU - Wang, Wen Juan

AU - Cheng, Wen Ping

AU - Yu, Xin Yu

AU - Yang, Jian Guo

AU - He, Ming Yuan

PY - 2008/1

Y1 - 2008/1

N2 - Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

AB - Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

KW - Fe-MCM-41

KW - Ionic liquid

KW - Mesoporous molecular sieves

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U2 - 10.3724/SP.J.1077.2008.00171

DO - 10.3724/SP.J.1077.2008.00171

M3 - 文章

AN - SCOPUS:39749177122

SN - 1000-324X

VL - 23

SP - 171

EP - 174

JO - Wuji Cailiao Xuebao/Journal of Inorganic Materials

JF - Wuji Cailiao Xuebao/Journal of Inorganic Materials

IS - 1

ER -

Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

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