Recycle waste salt as reagent: A one-pot substitution/Krapcho reaction sequence to -fluorinated esters and sulfones

Feng Zhu; Peng Wei Xu; Feng Zhou; Cui Hong Wang; Jian Zhou

doi:10.1021/acs.orglett.5b00072

Recycle waste salt as reagent: A one-pot substitution/Krapcho reaction sequence to -fluorinated esters and sulfones

Feng Zhu
, Peng Wei Xu
, Feng Zhou
, Cui Hong Wang^*
, Jian Zhou

^*此作品的通讯作者

化学与分子工程学院

East China Normal University
Nankai University

科研成果: 期刊稿件 › 文章 › 同行评审

40 引用（Scopus）

摘要

A "one-pot"tandem substitution/Krapcho reaction is reported for the facile synthesis of α-fluorinated esters and sulfones, which utilizes the byproduct salt formed in the substitution step as an indispensible reagent to facilitate the Krapcho reaction step. This represents the first sustainable tandem reaction that internally recycles the waste salt formed in the upstream step as the reagent for the downstream step.

源语言	英语
页（从-至）	972-975
页数	4
期刊	Organic Letters
卷	17
期	4
DOI	https://doi.org/10.1021/acs.orglett.5b00072
出版状态	已出版 - 20 2月 2015

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10.1021/acs.orglett.5b00072

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AU - Wang, Cui Hong

AU - Zhou, Jian

PY - 2015/2/20

Y1 - 2015/2/20

N2 - A "one-pot"tandem substitution/Krapcho reaction is reported for the facile synthesis of α-fluorinated esters and sulfones, which utilizes the byproduct salt formed in the substitution step as an indispensible reagent to facilitate the Krapcho reaction step. This represents the first sustainable tandem reaction that internally recycles the waste salt formed in the upstream step as the reagent for the downstream step.

AB - A "one-pot"tandem substitution/Krapcho reaction is reported for the facile synthesis of α-fluorinated esters and sulfones, which utilizes the byproduct salt formed in the substitution step as an indispensible reagent to facilitate the Krapcho reaction step. This represents the first sustainable tandem reaction that internally recycles the waste salt formed in the upstream step as the reagent for the downstream step.

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Recycle waste salt as reagent: A one-pot substitution/Krapcho reaction sequence to -fluorinated esters and sulfones

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