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Mechanochemical synthesis and characteristics of Pb(Mg1/3Nb 2/3)O3

  • Hao Wu*
  • , Cheng Chen
  • , Danyu Jiang
  • , Tao Feng
  • , Qiang Li
  • *此作品的通讯作者
  • East China Normal University
  • CAS - Shanghai Institute of Ceramics

科研成果: 书/报告/会议事项章节会议稿件同行评审

摘要

This paper presents a novel mechanochemical synthesis technique for making nano-structured Pb(Mg1/3Nb2/3)O3 (PMN) ferroelectric material without annealing treatment in a much shorter time and at much lower temperature than those reported in the literature, by using the starting precursors MgO, PbO, and Nb2O5. Specimens of various milling time (3-6h) are characterized from XRD patterns to track and analyze the synthesizing procedure of this mechanochemical processing route. The time used to make the desired PMN powders varies with different milling power. When the constituent oxides were mechanically activated at 1.8KW milling power for 6h, the perovskite phase PMN powder was obtained; while it was formed when milling at 3KW for only 3h. Typical SEM images of the as-received PMN powders show that the powders are aggregated of nano-particles of about 100nm in size.

源语言英语
主期刊名Testing and Evaluation of Inorganic Materials I
29-31
页数3
DOI
出版状态已出版 - 2011
活动1st Annual Meeting on Testing and Evaluation of Inorganic Materials - Nanchang, 中国
期限: 28 4月 201030 4月 2010

出版系列

姓名Advanced Materials Research
177
ISSN(印刷版)1022-6680

会议

会议1st Annual Meeting on Testing and Evaluation of Inorganic Materials
国家/地区中国
Nanchang
时期28/04/1030/04/10

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