A convenient synthesis of gimeracil

Xiao Lin Li; Hao Ting Zhu; Li Zhan; Ting Liu; Guang Cheng; Ning Liu; Shan Bao Yu; Hui Li; Yu Luo; Fan Yang; Jie Tang

doi:10.3184/174751918X15166150010920

A convenient synthesis of gimeracil

Xiao Lin Li
, Hao Ting Zhu
, Li Zhan
, Ting Liu
, Guang Cheng
, Ning Liu
, Shan Bao Yu
, Hui Li
, Yu Luo^*
, Fan Yang
, Jie Tang

^*此作品的通讯作者

化学与分子工程学院

科研成果: 期刊稿件 › 文章 › 同行评审

2 引用（Scopus）

摘要

A practical three-step synthetic approach to gimeracil in a 68% overall yield is described, using 2,4-dimethoxypyridine as the starting material with 3,5-dichloro-2,4-dimethoxypyridine and 3,5-dichloro-2,4-dihydroxypyridine as intermediates. The advantages of this procedure include short reaction steps, simple operation and good yield.

源语言	英语
页（从-至）	33-34
页数	2
期刊	Journal of Chemical Research
卷	42
期	1
DOI	https://doi.org/10.3184/174751918X15166150010920
出版状态	已出版 - 1月 2018

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10.3184/174751918X15166150010920

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title = "A convenient synthesis of gimeracil",

abstract = "A practical three-step synthetic approach to gimeracil in a 68\% overall yield is described, using 2,4-dimethoxypyridine as the starting material with 3,5-dichloro-2,4-dimethoxypyridine and 3,5-dichloro-2,4-dihydroxypyridine as intermediates. The advantages of this procedure include short reaction steps, simple operation and good yield.",

keywords = "Gimeracil, Protodechlorination, S-1, SAr, Synthesis of gimeracil",

author = "Li, \{Xiao Lin\} and Zhu, \{Hao Ting\} and Li Zhan and Ting Liu and Guang Cheng and Ning Liu and Yu, \{Shan Bao\} and Hui Li and Yu Luo and Fan Yang and Jie Tang",

year = "2018",

month = jan,

doi = "10.3184/174751918X15166150010920",

language = "英语",

volume = "42",

pages = "33--34",

journal = "Journal of Chemical Research",

issn = "1747-5198",

publisher = "Science Reviews Ltd",

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TY - JOUR

T1 - A convenient synthesis of gimeracil

AU - Li, Xiao Lin

AU - Zhu, Hao Ting

AU - Zhan, Li

AU - Liu, Ting

AU - Cheng, Guang

AU - Liu, Ning

AU - Yu, Shan Bao

AU - Li, Hui

AU - Luo, Yu

AU - Yang, Fan

AU - Tang, Jie

PY - 2018/1

Y1 - 2018/1

N2 - A practical three-step synthetic approach to gimeracil in a 68% overall yield is described, using 2,4-dimethoxypyridine as the starting material with 3,5-dichloro-2,4-dimethoxypyridine and 3,5-dichloro-2,4-dihydroxypyridine as intermediates. The advantages of this procedure include short reaction steps, simple operation and good yield.

AB - A practical three-step synthetic approach to gimeracil in a 68% overall yield is described, using 2,4-dimethoxypyridine as the starting material with 3,5-dichloro-2,4-dimethoxypyridine and 3,5-dichloro-2,4-dihydroxypyridine as intermediates. The advantages of this procedure include short reaction steps, simple operation and good yield.

KW - Gimeracil

KW - Protodechlorination

KW - S-1

KW - SAr

KW - Synthesis of gimeracil

UR - https://www.scopus.com/pages/publications/85042360369

U2 - 10.3184/174751918X15166150010920

DO - 10.3184/174751918X15166150010920

M3 - 文章

AN - SCOPUS:85042360369

SN - 1747-5198

VL - 42

SP - 33

EP - 34

JO - Journal of Chemical Research

JF - Journal of Chemical Research

IS - 1

ER -

A convenient synthesis of gimeracil

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