Synthesis and characterization the intercalation compound of SnS 2-ethylenediamine by hydrothermal reaction

Qing Lv, Caixia Li, Danyu Jiang, Qiang Li

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

2 Scopus citations

Abstract

The intercalation of ethylenediamine (en) into SnS2 was synthesised by hydrothermal reaction at the temperature of 180°C. And then dispersed the intercalation compounds in N, N-dimethylformamide (DMF) by stirring 48h, getting a light yellow sol, with the nature of uniform, transparent and stable. Analysised the structural of the product by means of X-ray powder diffraction (XRD). The morphology of sol was characterized by using of transmission electron microscopy (TEM). The UV-Vis spectrophotometer was utilized for the absorbance of the colloidal. The results show that en has been successfully inserted into the layer of tin disulphide, and the target products is of high purity and good crystal. The sol is of high stability and homogeneity, and have the strongest absorption at the Wavelength of 270nm.

Original languageEnglish
Title of host publicationHigh-Performance Ceramics VII
PublisherTrans Tech Publications Ltd
Pages215-218
Number of pages4
ISBN (Print)9783037854259
DOIs
StatePublished - 2012
Event7th China International Conference on High-Performance Ceramics, CICC-7 - Xiamen, China
Duration: 4 Nov 20117 Nov 2011

Publication series

NameKey Engineering Materials
Volume512-515
ISSN (Print)1013-9826
ISSN (Electronic)1662-9795

Conference

Conference7th China International Conference on High-Performance Ceramics, CICC-7
Country/TerritoryChina
CityXiamen
Period4/11/117/11/11

Keywords

  • Ethylenediamine
  • Hydrothermal
  • Intercalation compound
  • Tin disulfide

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