Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

Cai Hua Liu; Wen Juan Wang; Wen Ping Cheng; Xin Yu Yu; Jian Guo Yang; Ming Yuan He

doi:10.3724/SP.J.1077.2008.00171

Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

Cai Hua Liu^*
, Wen Juan Wang
, Wen Ping Cheng
, Xin Yu Yu
, Jian Guo Yang
, Ming Yuan He

^*Corresponding author for this work

School of Chemistry and Molecular Engineering

East China Normal University

Research output: Contribution to journal › Article › peer-review

5 Scopus citations

Abstract

Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C₁₆mim]⁺Br^-) as template at room temperature and characterized by X-ray diffraction, N₂ adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

Original language	English
Pages (from-to)	171-174
Number of pages	4
Journal	Wuji Cailiao Xuebao/Journal of Inorganic Materials
Volume	23
Issue number	1
DOIs	https://doi.org/10.3724/SP.J.1077.2008.00171
State	Published - Jan 2008

Keywords

Fe-MCM-41
Ionic liquid
Mesoporous molecular sieves

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10.3724/SP.J.1077.2008.00171

Cite this

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title = "Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41",

abstract = "Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.",

keywords = "Fe-MCM-41, Ionic liquid, Mesoporous molecular sieves",

author = "Liu, \{Cai Hua\} and Wang, \{Wen Juan\} and Cheng, \{Wen Ping\} and Yu, \{Xin Yu\} and Yang, \{Jian Guo\} and He, \{Ming Yuan\}",

year = "2008",

month = jan,

doi = "10.3724/SP.J.1077.2008.00171",

language = "英语",

volume = "23",

pages = "171--174",

journal = "Wuji Cailiao Xuebao/Journal of Inorganic Materials",

issn = "1000-324X",

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number = "1",

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TY - JOUR

T1 - Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

AU - Liu, Cai Hua

AU - Wang, Wen Juan

AU - Cheng, Wen Ping

AU - Yu, Xin Yu

AU - Yang, Jian Guo

AU - He, Ming Yuan

PY - 2008/1

Y1 - 2008/1

N2 - Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

AB - Mesoporous Fe-MCM-41 materials were synthesized by using ionic liquid 1-cethyl-3-methylimidazolium bromide ([C16mim]+Br-) as template at room temperature and characterized by X-ray diffraction, N2 adsorption-desorption, FT-IR, EPR, UV-Vis. Results show that these mesoporous materials possess high surface area. The pore size distributions of Fe-MCM-41 show that there are two types mesoporous. Part of iron atom still retain in the framework after removal of the template by calcination except those transferring to the wall surface. Fe species on wall surface are of high dispersion. This indicates that stable framework-iron containing mesoporous molecular sieves Fe-MCM-41 can be successfully synthesized.

KW - Fe-MCM-41

KW - Ionic liquid

KW - Mesoporous molecular sieves

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U2 - 10.3724/SP.J.1077.2008.00171

DO - 10.3724/SP.J.1077.2008.00171

M3 - 文章

AN - SCOPUS:39749177122

SN - 1000-324X

VL - 23

SP - 171

EP - 174

JO - Wuji Cailiao Xuebao/Journal of Inorganic Materials

JF - Wuji Cailiao Xuebao/Journal of Inorganic Materials

IS - 1

ER -

Synthesis and characterization of stable framework-iron containing mesoporous molecular sieves Fe-MCM-41

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Keywords

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