Surface modified Bi2SiO5 microflowers with Fe3+ doping for efficient degradation of organic contaminants

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Abstract

In this paper, a novel surface-doped Fe-Bi2SiO5 photocatalyst was synthesized by the oil bath method for the first time. Compared with the pure Bi2SiO5, the degradation rate constants of the FB-2 (the mole ratio of Fe/Bi was 1.7%) were increased by 3.8 and 5 times for Ciprofloxacin (CIP) and Rhodamine B (RhB), respectively. In addition, the results of the total organic carbon (TOC) test manifested that the mineralization capacity of FB-2 for CIP and RhB were increased to 40.7% and 64.7%, respectively. Moreover, the effects of catalyst dosage, initial solution concentration, initial pH and inorganic anions on photocatalytic performance were studied. The cyclic degradation experiments of FB-2 verified the excellent stability of photocatalysts, while active species trapping experiments and electron spin resonance (ESR) tests showed that superoxide radicals and holes played a major role in the degradation process. The paper presented that the photocatalytic activity of Bi-based photocatalysts was improved by a surface modified method, which provided a new idea for further study.

Original languageEnglish
Article number166866
JournalJournal of Alloys and Compounds
Volume926
DOIs
StatePublished - 10 Dec 2022
Externally publishedYes

Keywords

  • Fe-surface-doped BiSiO
  • Photocatalytic mechanism
  • Simulated sunlight driven
  • Surface modification

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