Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Qiang Wang; Julien Trébosc; Yixuan Li; Jun Xu; Bingwen Hu; Ningdong Feng; Qun Chen; Oliver Lafon; Jean Paul Amoureux; Feng Deng

doi:10.1039/c3cc42961j

Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Qiang Wang
, Julien Trébosc
, Yixuan Li
, Jun Xu
, Bingwen Hu
, Ningdong Feng
, Qun Chen
, Oliver Lafon
, Jean Paul Amoureux
, Feng Deng^*

^*Corresponding author for this work

School of Physics and Electronic Science

CAS - Innovation Academy for Precision Measurement Science and Technology
Université de Lille
East China Normal University

Research output: Contribution to journal › Article › peer-review

38 Scopus citations

Abstract

We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of ³¹P-(²⁷Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

Original language	English
Pages (from-to)	6653-6655
Number of pages	3
Journal	Chemical Communications
Volume	49
Issue number	59
DOIs	https://doi.org/10.1039/c3cc42961j
State	Published - 27 Jun 2013

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title = "Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei",

abstract = "We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.",

author = "Qiang Wang and Julien Tr{\'e}bosc and Yixuan Li and Jun Xu and Bingwen Hu and Ningdong Feng and Qun Chen and Oliver Lafon and Amoureux, \{Jean Paul\} and Feng Deng",

year = "2013",

month = jun,

day = "27",

doi = "10.1039/c3cc42961j",

language = "英语",

volume = "49",

pages = "6653--6655",

journal = "Chemical Communications",

issn = "1359-7345",

publisher = "Royal Society of Chemistry",

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TY - JOUR

T1 - Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

AU - Wang, Qiang

AU - Trébosc, Julien

AU - Li, Yixuan

AU - Xu, Jun

AU - Hu, Bingwen

AU - Feng, Ningdong

AU - Chen, Qun

AU - Lafon, Oliver

AU - Amoureux, Jean Paul

AU - Deng, Feng

PY - 2013/6/27

Y1 - 2013/6/27

N2 - We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

AB - We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

UR - https://www.scopus.com/pages/publications/84879757602

U2 - 10.1039/c3cc42961j

DO - 10.1039/c3cc42961j

M3 - 文章

AN - SCOPUS:84879757602

SN - 1359-7345

VL - 49

SP - 6653

EP - 6655

JO - Chemical Communications

JF - Chemical Communications

IS - 59

ER -

Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Abstract

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