Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Qiang Wang; Julien Trébosc; Yixuan Li; Jun Xu; Bingwen Hu; Ningdong Feng; Qun Chen; Oliver Lafon; Jean Paul Amoureux; Feng Deng

doi:10.1039/c3cc42961j

Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Qiang Wang, Julien Trébosc, Yixuan Li, Jun Xu, Bingwen Hu, Ningdong Feng, Qun Chen, Oliver Lafon, Jean Paul Amoureux, Feng Deng

School of Physics and Electronic Science

Research output: Contribution to journal › Article › peer-review

36 Scopus citations

Abstract

We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of ³¹P-(²⁷Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

Original language	English
Pages (from-to)	6653-6655
Number of pages	3
Journal	Chemical Communications
Volume	49
Issue number	59
DOIs	https://doi.org/10.1039/c3cc42961j
State	Published - 27 Jun 2013

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title = "Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei",

abstract = "We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.",

author = "Qiang Wang and Julien Tr{\'e}bosc and Yixuan Li and Jun Xu and Bingwen Hu and Ningdong Feng and Qun Chen and Oliver Lafon and Amoureux, \{Jean Paul\} and Feng Deng",

year = "2013",

month = jun,

day = "27",

doi = "10.1039/c3cc42961j",

language = "英语",

volume = "49",

pages = "6653--6655",

journal = "Chemical Communications",

issn = "1359-7345",

publisher = "Royal Society of Chemistry",

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TY - JOUR

T1 - Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

AU - Wang, Qiang

AU - Trébosc, Julien

AU - Li, Yixuan

AU - Xu, Jun

AU - Hu, Bingwen

AU - Feng, Ningdong

AU - Chen, Qun

AU - Lafon, Oliver

AU - Amoureux, Jean Paul

AU - Deng, Feng

PY - 2013/6/27

Y1 - 2013/6/27

N2 - We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

AB - We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-(27Al) J-HMQC experiments for a layered aluminophosphate Mu-4.

UR - https://www.scopus.com/pages/publications/84879757602

U2 - 10.1039/c3cc42961j

DO - 10.1039/c3cc42961j

M3 - 文章

AN - SCOPUS:84879757602

SN - 1359-7345

VL - 49

SP - 6653

EP - 6655

JO - Chemical Communications

JF - Chemical Communications

IS - 59

ER -

Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

Abstract

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