Selective C-O Bond Forming Reactions at Indole-C2-Position toward Polycyclic Indolone or Indolinone Derivatives Tethered with Medium-Sized Rings

  • Zongkang Wang
  • , Liqiang Yin
  • , Mengdan Wang
  • , Yilin Zhu
  • , Yajie Yang
  • , Lu Cheng
  • , Chengyu Wang*
  • , Yanzhong Li*
  • *Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

5 Scopus citations

Abstract

A methodology involving the chemoselective synthesis of tetracyclic [1,3]oxazino[3,2-a]indol-4-one or tetracyclic [1,3]oxazino[3,2-a]indoline-4-one tethered with a medium-sized ring by cross dehydrogenative coupling (CDC) or nucleophilic addition (NA) reaction has been developed. [1,3]Oxazino[3,2-a]indol-4-one compounds fused with a medium-sized ring were constructed through a CDC reaction in the presence of I2and K2CO3. Whereas, [1,3]oxazino[3,2-a]indoline-4-ones tethered with a medium-sized ring were obtained with a TfOH system by NA reaction.

Original languageEnglish
Pages (from-to)6272-6276
Number of pages5
JournalOrganic Letters
Volume24
Issue number34
DOIs
StatePublished - 2 Sep 2022

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