Regioselective synthesis and photooxygenations of furonaphthopyrones starting from 2,7-naphthalenediol

Zhi Fu Tao; Xuhong Qian; Mingcai Fan

doi:10.1016/S0040-4020(97)00845-4

Regioselective synthesis and photooxygenations of furonaphthopyrones starting from 2,7-naphthalenediol

Zhi Fu Tao, Xuhong Qian, Mingcai Fan

East China University of Science and Technology

Research output: Contribution to journal › Article › peer-review

26 Scopus citations

Abstract

Three angular furonaphthopyrones 4, 9, 12 were regioselectively synthesized starting from 2,7-naphthalenediol in three steps, respectively. An easy separation of Pechmann condensation products 1 and 2 of 2, 7-naphthalenediol with ethyl acetoacetate was described. The photooxygenations of 4, 12 were investigated and a hydroperoxide 18 was isolated and fully characterized.

Original language	English
Pages (from-to)	13329-13338
Number of pages	10
Journal	Tetrahedron
Volume	53
Issue number	39
DOIs	https://doi.org/10.1016/S0040-4020(97)00845-4
State	Published - 29 Sep 1997
Externally published	Yes

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title = "Regioselective synthesis and photooxygenations of furonaphthopyrones starting from 2,7-naphthalenediol",

abstract = "Three angular furonaphthopyrones 4, 9, 12 were regioselectively synthesized starting from 2,7-naphthalenediol in three steps, respectively. An easy separation of Pechmann condensation products 1 and 2 of 2, 7-naphthalenediol with ethyl acetoacetate was described. The photooxygenations of 4, 12 were investigated and a hydroperoxide 18 was isolated and fully characterized.",

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T1 - Regioselective synthesis and photooxygenations of furonaphthopyrones starting from 2,7-naphthalenediol

AU - Tao, Zhi Fu

AU - Qian, Xuhong

AU - Fan, Mingcai

PY - 1997/9/29

Y1 - 1997/9/29

N2 - Three angular furonaphthopyrones 4, 9, 12 were regioselectively synthesized starting from 2,7-naphthalenediol in three steps, respectively. An easy separation of Pechmann condensation products 1 and 2 of 2, 7-naphthalenediol with ethyl acetoacetate was described. The photooxygenations of 4, 12 were investigated and a hydroperoxide 18 was isolated and fully characterized.

AB - Three angular furonaphthopyrones 4, 9, 12 were regioselectively synthesized starting from 2,7-naphthalenediol in three steps, respectively. An easy separation of Pechmann condensation products 1 and 2 of 2, 7-naphthalenediol with ethyl acetoacetate was described. The photooxygenations of 4, 12 were investigated and a hydroperoxide 18 was isolated and fully characterized.

UR - https://www.scopus.com/pages/publications/0030768587

U2 - 10.1016/S0040-4020(97)00845-4

DO - 10.1016/S0040-4020(97)00845-4

M3 - 文章

AN - SCOPUS:0030768587

SN - 0040-4020

VL - 53

SP - 13329

EP - 13338

JO - Tetrahedron

JF - Tetrahedron

IS - 39

ER -

Regioselective synthesis and photooxygenations of furonaphthopyrones starting from 2,7-naphthalenediol

Abstract

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