Preparation of extra fine nano-sized MgO by precipitation and polymer protection method

Hai Xia Wang; Bing Yuan Hu; Lin Sheng Wang; Guang Da Yang; Qiang Li

Preparation of extra fine nano-sized MgO by precipitation and polymer protection method

Hai Xia Wang^*
, Bing Yuan Hu
, Lin Sheng Wang
, Guang Da Yang
, Qiang Li

^*Corresponding author for this work

School of Chemistry and Molecular Engineering

East China Normal University

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

The precursor for nano-sized magnesia was prepared by using Mg(NO ₃)₂·6H₂O as raw material, the hydrolysis product of hexamethylene tetramine as precipitating reagent and water as reaction media, and with the polymer (PEG) and DMF as protection reagents for particles. Nano-sized magnesia was prepared by calcining the precursor at 873 K after being dehydrated by freeze centrifugation and vacuum drying at a constant temperature. The formation process and structure of MgO nanocrystallites were investigated by means of TG-DTA, FTIR, TEM, XRD and BET. The results showed that the crystal belonged to cubic system and the average size was 3.1 nm and the specific surface area was 229 m²·g^-1.

Original language	English
Pages (from-to)	363-366
Number of pages	4
Journal	Chinese Journal of Inorganic Chemistry
Volume	22
Issue number	2
State	Published - Feb 2006

Keywords

Hexamethylene tetramine
Nano-sized magnesia
Polymer protection
Precipitation method

Cite this

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title = "Preparation of extra fine nano-sized MgO by precipitation and polymer protection method",

abstract = "The precursor for nano-sized magnesia was prepared by using Mg(NO 3)2·6H2O as raw material, the hydrolysis product of hexamethylene tetramine as precipitating reagent and water as reaction media, and with the polymer (PEG) and DMF as protection reagents for particles. Nano-sized magnesia was prepared by calcining the precursor at 873 K after being dehydrated by freeze centrifugation and vacuum drying at a constant temperature. The formation process and structure of MgO nanocrystallites were investigated by means of TG-DTA, FTIR, TEM, XRD and BET. The results showed that the crystal belonged to cubic system and the average size was 3.1 nm and the specific surface area was 229 m2·g-1.",

keywords = "Hexamethylene tetramine, Nano-sized magnesia, Polymer protection, Precipitation method",

author = "Wang, \{Hai Xia\} and Hu, \{Bing Yuan\} and Wang, \{Lin Sheng\} and Yang, \{Guang Da\} and Qiang Li",

year = "2006",

month = feb,

language = "英语",

volume = "22",

pages = "363--366",

journal = "Chinese Journal of Inorganic Chemistry",

issn = "1001-4861",

publisher = "Chinese Chemical Society",

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TY - JOUR

T1 - Preparation of extra fine nano-sized MgO by precipitation and polymer protection method

AU - Wang, Hai Xia

AU - Hu, Bing Yuan

AU - Wang, Lin Sheng

AU - Yang, Guang Da

AU - Li, Qiang

PY - 2006/2

Y1 - 2006/2

N2 - The precursor for nano-sized magnesia was prepared by using Mg(NO 3)2·6H2O as raw material, the hydrolysis product of hexamethylene tetramine as precipitating reagent and water as reaction media, and with the polymer (PEG) and DMF as protection reagents for particles. Nano-sized magnesia was prepared by calcining the precursor at 873 K after being dehydrated by freeze centrifugation and vacuum drying at a constant temperature. The formation process and structure of MgO nanocrystallites were investigated by means of TG-DTA, FTIR, TEM, XRD and BET. The results showed that the crystal belonged to cubic system and the average size was 3.1 nm and the specific surface area was 229 m2·g-1.

AB - The precursor for nano-sized magnesia was prepared by using Mg(NO 3)2·6H2O as raw material, the hydrolysis product of hexamethylene tetramine as precipitating reagent and water as reaction media, and with the polymer (PEG) and DMF as protection reagents for particles. Nano-sized magnesia was prepared by calcining the precursor at 873 K after being dehydrated by freeze centrifugation and vacuum drying at a constant temperature. The formation process and structure of MgO nanocrystallites were investigated by means of TG-DTA, FTIR, TEM, XRD and BET. The results showed that the crystal belonged to cubic system and the average size was 3.1 nm and the specific surface area was 229 m2·g-1.

KW - Hexamethylene tetramine

KW - Nano-sized magnesia

KW - Polymer protection

KW - Precipitation method

UR - https://www.scopus.com/pages/publications/31644435918

M3 - 文章

AN - SCOPUS:31644435918

SN - 1001-4861

VL - 22

SP - 363

EP - 366

JO - Chinese Journal of Inorganic Chemistry

JF - Chinese Journal of Inorganic Chemistry

IS - 2

ER -

Preparation of extra fine nano-sized MgO by precipitation and polymer protection method

Abstract

Keywords

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