Poly(ionic liquid)s-Supported N-Heterocyclic Carbene Silver Complexes for the Cycloaddition of CO2 with Epoxides

  • Li Qin
  • , Yayan Ji
  • , Tong Ding
  • , Bo Liu
  • , Rong Wang
  • , Liangzheng Ji
  • , Guohua Gao*
  • *Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

18 Scopus citations

Abstract

Abstract: A series of poly(ionic liquid)s-supported N-heterocyclic carbene silver complexes (Poly(NHC-Ag/IL)s), poly(ionic liquid)s (PILs) and poly(N-heterocyclic carbene silver complexes) (Poly(NHC-Ag)s) were prepared through radical co-polymerization of N-vinylimidazolium ionic liquids, NHC-Ag monomers and divinylbenzene, respectively. These polymers were applied to catalyze the cycloaddition reaction of carbon dioxide and epoxides without any co-catalyst. Poly(NHC-Ag/IL)s exhibited higher activities than the corresponding PILs and Poly(NHC-Ag)s, which was attributed to the synergistic effect of NHC-Ag and bromide. Furthermore, Poly(NHC-Ag/IL)s could be easily recycled five times without significant loss of catalytic activity. Graphic Abstract: Multi-functional poly(ionic liquid)s-supported N-heterocyclic carbene silver complexes (Poly(NHC-Ag/IL)s) were synthesized by radical co-polymerization of N-vinylimidazolium ionic liquids, NHC-Ag monomers and DVB. Poly(NHC-Ag/IL)s exhibited high activities for cycloaddition reaction of carbon dioxide and epoxides due to their multi-functional groups including Lewis acidic silver and a bromine anion.

Original languageEnglish
Pages (from-to)1196-1203
Number of pages8
JournalCatalysis Letters
Volume150
Issue number4
DOIs
StatePublished - 1 Apr 2020

Keywords

  • Carbon dioxide
  • Cycloaddition reaction
  • NHC-Ag
  • Poly(ionic liquid)s
  • Synergistic catalysis

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