Parameter control in the synthesis of ordered porous zirconium oxide

Hang Rong Chen; Jian Lin Shi; Zi Le Hua; Mei Ling Ruan; Dong Sheng Yan

doi:10.1016/S0167-577X(01)00286-5

Parameter control in the synthesis of ordered porous zirconium oxide

Hang Rong Chen
, Jian Lin Shi^*
, Zi Le Hua
, Mei Ling Ruan
, Dong Sheng Yan

^*Corresponding author for this work

CAS - Shanghai Institute of Ceramics

Research output: Contribution to journal › Article › peer-review

21 Scopus citations

Abstract

The ordered porous zirconium oxide with thermal stability up to 600°C has been synthesized by a surfactant-assisted route and a post-synthetic treatment with phosphoric acid. XRD, N₂ adsorption, HRTEM and UV-VIS spectroscopy were adopted for the characterization of the synthesized sample. It was shown that the parameter control, including the lower molar ratio of surfactant to zirconium resource (0.2-0.3), higher hydrothermal temperature (110°C), and the suitable H₃PO₄ concentration (0.2-0.3 M), is important for the synthesis of high-quality zirconium oxide material with ordered pore structure.

Original language	English
Pages (from-to)	187-193
Number of pages	7
Journal	Materials Letters
Volume	51
Issue number	3
DOIs	https://doi.org/10.1016/S0167-577X(01)00286-5
State	Published - Nov 2001
Externally published	Yes

Keywords

Ordered porous zirconium oxide
Parameter control
Phosphoric acid (post-treatment)

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10.1016/S0167-577X(01)00286-5

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title = "Parameter control in the synthesis of ordered porous zirconium oxide",

abstract = "The ordered porous zirconium oxide with thermal stability up to 600°C has been synthesized by a surfactant-assisted route and a post-synthetic treatment with phosphoric acid. XRD, N2 adsorption, HRTEM and UV-VIS spectroscopy were adopted for the characterization of the synthesized sample. It was shown that the parameter control, including the lower molar ratio of surfactant to zirconium resource (0.2-0.3), higher hydrothermal temperature (110°C), and the suitable H3PO4 concentration (0.2-0.3 M), is important for the synthesis of high-quality zirconium oxide material with ordered pore structure.",

keywords = "Ordered porous zirconium oxide, Parameter control, Phosphoric acid (post-treatment)",

author = "Chen, \{Hang Rong\} and Shi, \{Jian Lin\} and Hua, \{Zi Le\} and Ruan, \{Mei Ling\} and Yan, \{Dong Sheng\}",

year = "2001",

month = nov,

doi = "10.1016/S0167-577X(01)00286-5",

language = "英语",

volume = "51",

pages = "187--193",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier B.V.",

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TY - JOUR

T1 - Parameter control in the synthesis of ordered porous zirconium oxide

AU - Chen, Hang Rong

AU - Shi, Jian Lin

AU - Hua, Zi Le

AU - Ruan, Mei Ling

AU - Yan, Dong Sheng

PY - 2001/11

Y1 - 2001/11

N2 - The ordered porous zirconium oxide with thermal stability up to 600°C has been synthesized by a surfactant-assisted route and a post-synthetic treatment with phosphoric acid. XRD, N2 adsorption, HRTEM and UV-VIS spectroscopy were adopted for the characterization of the synthesized sample. It was shown that the parameter control, including the lower molar ratio of surfactant to zirconium resource (0.2-0.3), higher hydrothermal temperature (110°C), and the suitable H3PO4 concentration (0.2-0.3 M), is important for the synthesis of high-quality zirconium oxide material with ordered pore structure.

AB - The ordered porous zirconium oxide with thermal stability up to 600°C has been synthesized by a surfactant-assisted route and a post-synthetic treatment with phosphoric acid. XRD, N2 adsorption, HRTEM and UV-VIS spectroscopy were adopted for the characterization of the synthesized sample. It was shown that the parameter control, including the lower molar ratio of surfactant to zirconium resource (0.2-0.3), higher hydrothermal temperature (110°C), and the suitable H3PO4 concentration (0.2-0.3 M), is important for the synthesis of high-quality zirconium oxide material with ordered pore structure.

KW - Ordered porous zirconium oxide

KW - Parameter control

KW - Phosphoric acid (post-treatment)

UR - https://www.scopus.com/pages/publications/0035498478

U2 - 10.1016/S0167-577X(01)00286-5

DO - 10.1016/S0167-577X(01)00286-5

M3 - 文章

AN - SCOPUS:0035498478

SN - 0167-577X

VL - 51

SP - 187

EP - 193

JO - Materials Letters

JF - Materials Letters

IS - 3

ER -

Parameter control in the synthesis of ordered porous zirconium oxide

Abstract

Keywords

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