Observing 13C-13C connectivities at high magnetic fields and very high spinning frequencies

Olivier Lafon; Julien Trébosc; Bingwen Hu; Gaël De Paëpe; Jean Paul Amoureux

doi:10.1039/c1cc11705j

Observing ¹³C-¹³C connectivities at high magnetic fields and very high spinning frequencies

Olivier Lafon, Julien Trébosc, Bingwen Hu, Gaël De Paëpe, Jean Paul Amoureux

School of Physics and Electronic Science

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

We report the application of a dipolar recoupling sequence for the observation of ¹³C-¹³C connectivities in biomolecules at high magnetic fields (B₀ ≥ 21.1 T) and ultra-high magic angle spinning frequencies (ν_R = 60 kHz). The efficiency and the robustness of this double-quantum technique are demonstrated on the YajG protein (19.6 kDa).

Original language	English
Pages (from-to)	6930-6932
Number of pages	3
Journal	Chemical Communications
Volume	47
Issue number	24
DOIs	https://doi.org/10.1039/c1cc11705j
State	Published - 2011

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10.1039/c1cc11705j

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title = "Observing 13C-13C connectivities at high magnetic fields and very high spinning frequencies",

abstract = "We report the application of a dipolar recoupling sequence for the observation of 13C-13C connectivities in biomolecules at high magnetic fields (B0 ≥ 21.1 T) and ultra-high magic angle spinning frequencies (νR = 60 kHz). The efficiency and the robustness of this double-quantum technique are demonstrated on the YajG protein (19.6 kDa).",

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AU - Lafon, Olivier

AU - Trébosc, Julien

AU - Hu, Bingwen

AU - Paëpe, Gaël De

AU - Amoureux, Jean Paul

PY - 2011

Y1 - 2011

N2 - We report the application of a dipolar recoupling sequence for the observation of 13C-13C connectivities in biomolecules at high magnetic fields (B0 ≥ 21.1 T) and ultra-high magic angle spinning frequencies (νR = 60 kHz). The efficiency and the robustness of this double-quantum technique are demonstrated on the YajG protein (19.6 kDa).

AB - We report the application of a dipolar recoupling sequence for the observation of 13C-13C connectivities in biomolecules at high magnetic fields (B0 ≥ 21.1 T) and ultra-high magic angle spinning frequencies (νR = 60 kHz). The efficiency and the robustness of this double-quantum technique are demonstrated on the YajG protein (19.6 kDa).

UR - https://www.scopus.com/pages/publications/79959798005

U2 - 10.1039/c1cc11705j

DO - 10.1039/c1cc11705j

M3 - 文章

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AN - SCOPUS:79959798005

SN - 1359-7345

VL - 47

SP - 6930

EP - 6932

JO - Chemical Communications

JF - Chemical Communications

IS - 24

ER -

Observing ¹³C-¹³C connectivities at high magnetic fields and very high spinning frequencies

Abstract

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