Novel phase transformation phenomenon of potassium teteratitanate nanofibres synthesized from H2TiO3

Na Zhang; Haifang Xu; Yulin Li; Qiang Li; Cheng Zhang

doi:10.4028/www.scientific.net/AMR.177.62

Novel phase transformation phenomenon of potassium teteratitanate nanofibres synthesized from H₂TiO₃

Na Zhang^*
, Haifang Xu
, Yulin Li
, Qiang Li
, Cheng Zhang

^*Corresponding author for this work

School of Chemistry and Molecular Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Starting from H₂TiO₃, potassium teteratitanate (K₂Ti₄O₉) nanofibres with the length of several micrometers and the diameter of 100nm were directly synthesized by solid state reaction. The novel phase transformation and structure change behavior was investigated by the X-ray diffraction technique (XRD), scanning electron microscopy (SEM) in details. In series of hydrothermal reaction, the K ₂Ti₄O₉ could transfer to anatase TiO ₂ and rutile TiO₂. Aggregated anatase TiO₂ particles and rod-like rutile TiO₂ were produced respectively in 1M HCl solutions at 160°C and 220°C. When the 0.01M HCl solution was considered as solvent, the mixture of floral anatase TiO₂ and K ₂Ti₄O₉ were present together.

Original language	English
Title of host publication	Testing and Evaluation of Inorganic Materials I
Pages	62-65
Number of pages	4
DOIs	https://doi.org/10.4028/www.scientific.net/AMR.177.62
State	Published - 2011
Event	1st Annual Meeting on Testing and Evaluation of Inorganic Materials - Nanchang, China Duration: 28 Apr 2010 → 30 Apr 2010

Publication series

Name	Advanced Materials Research
Volume	177
ISSN (Print)	1022-6680

Conference

Conference	1st Annual Meeting on Testing and Evaluation of Inorganic Materials
Country/Territory	China
City	Nanchang
Period	28/04/10 → 30/04/10

Keywords

Hydrothermal reaction
Nanofibres
Nanorod
Phase transformation

Access to Document

10.4028/www.scientific.net/AMR.177.62

Cite this

@inproceedings{d9cf30bb923042d48c9b2e605c766323,

title = "Novel phase transformation phenomenon of potassium teteratitanate nanofibres synthesized from H2TiO3",

abstract = "Starting from H2TiO3, potassium teteratitanate (K2Ti4O9) nanofibres with the length of several micrometers and the diameter of 100nm were directly synthesized by solid state reaction. The novel phase transformation and structure change behavior was investigated by the X-ray diffraction technique (XRD), scanning electron microscopy (SEM) in details. In series of hydrothermal reaction, the K 2Ti4O9 could transfer to anatase TiO 2 and rutile TiO2. Aggregated anatase TiO2 particles and rod-like rutile TiO2 were produced respectively in 1M HCl solutions at 160°C and 220°C. When the 0.01M HCl solution was considered as solvent, the mixture of floral anatase TiO2 and K 2Ti4O9 were present together.",

keywords = "Hydrothermal reaction, Nanofibres, Nanorod, Phase transformation",

author = "Na Zhang and Haifang Xu and Yulin Li and Qiang Li and Cheng Zhang",

year = "2011",

doi = "10.4028/www.scientific.net/AMR.177.62",

language = "英语",

isbn = "9783037850138",

series = "Advanced Materials Research",

pages = "62--65",

booktitle = "Testing and Evaluation of Inorganic Materials I",

note = "1st Annual Meeting on Testing and Evaluation of Inorganic Materials ; Conference date: 28-04-2010 Through 30-04-2010",

}

Zhang, N, Xu, H, Li, Y, Li, Q & Zhang, C 2011, Novel phase transformation phenomenon of potassium teteratitanate nanofibres synthesized from H₂TiO₃. in Testing and Evaluation of Inorganic Materials I. Advanced Materials Research, vol. 177, pp. 62-65, 1st Annual Meeting on Testing and Evaluation of Inorganic Materials, Nanchang, China, 28/04/10. https://doi.org/10.4028/www.scientific.net/AMR.177.62

TY - GEN

T1 - Novel phase transformation phenomenon of potassium teteratitanate nanofibres synthesized from H2TiO3

AU - Zhang, Na

AU - Xu, Haifang

AU - Li, Yulin

AU - Li, Qiang

AU - Zhang, Cheng

PY - 2011

Y1 - 2011

N2 - Starting from H2TiO3, potassium teteratitanate (K2Ti4O9) nanofibres with the length of several micrometers and the diameter of 100nm were directly synthesized by solid state reaction. The novel phase transformation and structure change behavior was investigated by the X-ray diffraction technique (XRD), scanning electron microscopy (SEM) in details. In series of hydrothermal reaction, the K 2Ti4O9 could transfer to anatase TiO 2 and rutile TiO2. Aggregated anatase TiO2 particles and rod-like rutile TiO2 were produced respectively in 1M HCl solutions at 160°C and 220°C. When the 0.01M HCl solution was considered as solvent, the mixture of floral anatase TiO2 and K 2Ti4O9 were present together.

AB - Starting from H2TiO3, potassium teteratitanate (K2Ti4O9) nanofibres with the length of several micrometers and the diameter of 100nm were directly synthesized by solid state reaction. The novel phase transformation and structure change behavior was investigated by the X-ray diffraction technique (XRD), scanning electron microscopy (SEM) in details. In series of hydrothermal reaction, the K 2Ti4O9 could transfer to anatase TiO 2 and rutile TiO2. Aggregated anatase TiO2 particles and rod-like rutile TiO2 were produced respectively in 1M HCl solutions at 160°C and 220°C. When the 0.01M HCl solution was considered as solvent, the mixture of floral anatase TiO2 and K 2Ti4O9 were present together.

KW - Hydrothermal reaction

KW - Nanofibres

KW - Nanorod

KW - Phase transformation

UR - https://www.scopus.com/pages/publications/78751561610

U2 - 10.4028/www.scientific.net/AMR.177.62

DO - 10.4028/www.scientific.net/AMR.177.62

M3 - 会议稿件

AN - SCOPUS:78751561610

SN - 9783037850138

T3 - Advanced Materials Research

SP - 62

EP - 65

BT - Testing and Evaluation of Inorganic Materials I

T2 - 1st Annual Meeting on Testing and Evaluation of Inorganic Materials

Y2 - 28 April 2010 through 30 April 2010

ER -