Homonuclear dipolar decoupling schemes for fast MAS

Jean Paul Amoureux; Bingwen Hu; Julien Trébosc; Qiang Wang; Olivier Lafon; Feng Deng

doi:10.1016/j.ssnmr.2008.10.006

Homonuclear dipolar decoupling schemes for fast MAS

Jean Paul Amoureux^*
, Bingwen Hu
, Julien Trébosc
, Qiang Wang
, Olivier Lafon
, Feng Deng

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

27 Scopus citations

Abstract

We present two one-dimensional methods that allow direct observation of highly resolved ¹H spectra in solid-state NMR. The methods, which work mainly at 30-35 kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.

Original language	English
Pages (from-to)	19-24
Number of pages	6
Journal	Solid State Nuclear Magnetic Resonance
Volume	35
Issue number	1
DOIs	https://doi.org/10.1016/j.ssnmr.2008.10.006
State	Published - Feb 2009
Externally published	Yes

Keywords

1D NMR
H high-resolution
Solid-state NMR
Ultra-fast MAS

Access to Document

10.1016/j.ssnmr.2008.10.006

Cite this

@article{b2034191db7b4424b12a7bd97aad42bc,

title = "Homonuclear dipolar decoupling schemes for fast MAS",

abstract = "We present two one-dimensional methods that allow direct observation of highly resolved 1H spectra in solid-state NMR. The methods, which work mainly at 30-35 kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.",

keywords = "1D NMR, H high-resolution, Solid-state NMR, Ultra-fast MAS",

author = "Amoureux, \{Jean Paul\} and Bingwen Hu and Julien Tr{\'e}bosc and Qiang Wang and Olivier Lafon and Feng Deng",

year = "2009",

month = feb,

doi = "10.1016/j.ssnmr.2008.10.006",

language = "英语",

volume = "35",

pages = "19--24",

journal = "Solid State Nuclear Magnetic Resonance",

issn = "0926-2040",

publisher = "Elsevier B.V.",

number = "1",

}

TY - JOUR

T1 - Homonuclear dipolar decoupling schemes for fast MAS

AU - Amoureux, Jean Paul

AU - Hu, Bingwen

AU - Trébosc, Julien

AU - Wang, Qiang

AU - Lafon, Olivier

AU - Deng, Feng

PY - 2009/2

Y1 - 2009/2

N2 - We present two one-dimensional methods that allow direct observation of highly resolved 1H spectra in solid-state NMR. The methods, which work mainly at 30-35 kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.

AB - We present two one-dimensional methods that allow direct observation of highly resolved 1H spectra in solid-state NMR. The methods, which work mainly at 30-35 kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.

KW - 1D NMR

KW - H high-resolution

KW - Solid-state NMR

KW - Ultra-fast MAS

UR - https://www.scopus.com/pages/publications/58849159099

U2 - 10.1016/j.ssnmr.2008.10.006

DO - 10.1016/j.ssnmr.2008.10.006

M3 - 文章

C2 - 19101127

AN - SCOPUS:58849159099

SN - 0926-2040

VL - 35

SP - 19

EP - 24

JO - Solid State Nuclear Magnetic Resonance

JF - Solid State Nuclear Magnetic Resonance

IS - 1

ER -

Homonuclear dipolar decoupling schemes for fast MAS

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this