Highly efficient procedure for the oxathioacetalization of carbonyl compounds under solvent-free conditions

Xuezheng Liang; Shan Gao; Jianguo Yang; Mingyuan He

doi:10.1016/j.catcom.2008.08.008

Highly efficient procedure for the oxathioacetalization of carbonyl compounds under solvent-free conditions

Xuezheng Liang, Shan Gao, Jianguo Yang, Mingyuan He

School of Chemistry and Molecular Engineering

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

The novel efficient procedure has been developed for the oxathioacetalization of carbonyl compounds and 2-mercaptoethanol under solvent-free condition at room temperature. The results showed that the novel catalyst was very efficient for the reaction with the average yield over 90%. Operational simplicity, without need of any solvent, small amount of usage, low cost of the catalyst used, high yields, applicability to large-scale reactions, reusability and chemoselectivity are the key features of this methodology.

Original language	English
Pages (from-to)	156-159
Number of pages	4
Journal	Catalysis Communications
Volume	10
Issue number	2
DOIs	https://doi.org/10.1016/j.catcom.2008.08.008
State	Published - 15 Nov 2008

Keywords

Catalysis
Chemoselective
Efficient
Oxathioacetalization

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10.1016/j.catcom.2008.08.008

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title = "Highly efficient procedure for the oxathioacetalization of carbonyl compounds under solvent-free conditions",

abstract = "The novel efficient procedure has been developed for the oxathioacetalization of carbonyl compounds and 2-mercaptoethanol under solvent-free condition at room temperature. The results showed that the novel catalyst was very efficient for the reaction with the average yield over 90\%. Operational simplicity, without need of any solvent, small amount of usage, low cost of the catalyst used, high yields, applicability to large-scale reactions, reusability and chemoselectivity are the key features of this methodology.",

keywords = "Catalysis, Chemoselective, Efficient, Oxathioacetalization",

author = "Xuezheng Liang and Shan Gao and Jianguo Yang and Mingyuan He",

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AU - Liang, Xuezheng

AU - Gao, Shan

AU - Yang, Jianguo

AU - He, Mingyuan

PY - 2008/11/15

Y1 - 2008/11/15

N2 - The novel efficient procedure has been developed for the oxathioacetalization of carbonyl compounds and 2-mercaptoethanol under solvent-free condition at room temperature. The results showed that the novel catalyst was very efficient for the reaction with the average yield over 90%. Operational simplicity, without need of any solvent, small amount of usage, low cost of the catalyst used, high yields, applicability to large-scale reactions, reusability and chemoselectivity are the key features of this methodology.

AB - The novel efficient procedure has been developed for the oxathioacetalization of carbonyl compounds and 2-mercaptoethanol under solvent-free condition at room temperature. The results showed that the novel catalyst was very efficient for the reaction with the average yield over 90%. Operational simplicity, without need of any solvent, small amount of usage, low cost of the catalyst used, high yields, applicability to large-scale reactions, reusability and chemoselectivity are the key features of this methodology.

KW - Catalysis

KW - Chemoselective

KW - Efficient

KW - Oxathioacetalization

UR - https://www.scopus.com/pages/publications/54049146209

U2 - 10.1016/j.catcom.2008.08.008

DO - 10.1016/j.catcom.2008.08.008

M3 - 文章

AN - SCOPUS:54049146209

SN - 1566-7367

VL - 10

SP - 156

EP - 159

JO - Catalysis Communications

JF - Catalysis Communications

IS - 2

ER -

Highly efficient procedure for the oxathioacetalization of carbonyl compounds under solvent-free conditions

Abstract

Keywords

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