Abstract
The [Zr(OH)5]-imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO2 by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO2 nanostructures.
| Original language | English |
|---|---|
| Pages (from-to) | 362-365 |
| Number of pages | 4 |
| Journal | International Journal of Materials Research |
| Volume | 109 |
| Issue number | 4 |
| DOIs | |
| State | Published - Apr 2018 |
Keywords
- Anion exchange reaction
- Ionic liquid
- Nanoplate
- Zirconia precursor
- Zirconium oxide