Exploration of 1,3-dipolar cycloaddition reactions to construct the core skeleton of Calyciphylline A-type alkaloids

Jiaxin Zhong, Haibing He, Shuanhu Gao

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Abstract

Nitrone induced 1,3-dipolar [3 + 2] cycloadditions were studied to construct the core structure of Calyciphylline A-type Daphniphyllum alkaloids. This approach is capable of installing the cis-hydroindole A-C ring as well as the spiro-A-C-E ring with the all-carbon quaternary centers at C-5 and C-8, and has been successfully used in the total synthesis of himalensine A. It also lays the foundation for the synthesis of challenging Calyciphylline A-type alkaloids, such as daphniyunnine A.

Original languageEnglish
Pages (from-to)3781-3785
Number of pages5
JournalOrganic Chemistry Frontiers
Volume6
Issue number22
DOIs
StatePublished - 21 Nov 2019

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