Enhanced photoelectrochemical activity of ZnO-coated TiO2 nanotubes and its dependence on ZnO coating thickness

  • Hua Cai
  • , Peipei Liang
  • , Zhigao Hu
  • , Liqun Shi
  • , Xu Yang
  • , Jian Sun
  • , Ning Xu
  • , Jiada Wu*
  • *Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

43 Scopus citations

Abstract

One-dimensional heterogeneous nanostructures in the form of ZnO-coated TiO2 nanotubes (ZnO/TiO2 NTs) were fabricated by atomic layer deposition of an ultrathin ZnO coating on electrochemical anodization-formed TiO2 nanotubes (NTs) with the thickness of ZnO coating being precisely controlled at atomic scale, and the photoelectrochemical activity of the fabricated ZnO/TiO2 NTs and the influence of ZnO coating and its thickness were studied. The structures of TiO2 NTs and ZnO coatings were characterized by X-ray diffraction, Raman backscattering spectroscopy, and transmission electron microscopy. The photoelectrochemical activity was studied through the measurements of electrochemical impendence, flat-band potential, and transient photocurrent density. The TiO2 NTs exhibit anatase structure, and the ZnO coatings are structured with hexagonal wurtzite. The photoelectrochemical activity of the ZnO/TiO2 NTs is strongly dependent on the thickness of ZnO coating. ZnO/ TiO2 NTs with a thinner rather than a thicker ZnO coating exhibit better photoelectrochemical activity with reduced charge transfer resistance, increased negative flat-band potentials, and enhanced photocurrent densities. Under visible illumination, an increase of about 60 % in the photoelectrochemical activity is obtained for ZnO/TiO2 NTs with an about 2-nm-thick ZnO coating.

Original languageEnglish
Article number104
JournalNanoscale Research Letters
Volume11
Issue number1
DOIs
StatePublished - 2016

Keywords

  • Heterogeneous nanostructure
  • Photoelectrochemical activity
  • TiO
  • ZnO
  • ZnO-coated TiO nanotube

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