Effect of synthesis conditions on luminescence properties of PbWO 4 nanospheres and nanoflakes

M. M. Li; Q. S. Wu; J. L. Shi

doi:10.1179/175355509X460631

Effect of synthesis conditions on luminescence properties of PbWO ₄ nanospheres and nanoflakes

M. M. Li, Q. S. Wu, J. L. Shi

Research output: Contribution to journal › Article › peer-review

3 Scopus citations

Abstract

Lead tungstate (PbWO₄) nanospheres and nanoflakes have been prepared by template directed synthesis using a biotemplate based on a new egg shell. The product was characterised by X-ray diffraction, scanning electron microscopy and luminescence spectrophotometer. The product morphology could be transformed from nanospheres to nanoflakes via a simple change of solvent. A green emission peak at 480 nm was observed for the flake PbWO₄, whereas the emission peak was blue for the PbWO₄ nanospheres. The effect of solvent type on the morphology and properties of the synthesised PbWO₄ was investigated and a possible formation mechanism for nanospheres or sheets is proposed. The PbWO₄ nanocrystals have potential optical applications.

Original language	English
Pages (from-to)	108-110
Number of pages	3
Journal	Materials Technology
Volume	24
Issue number	2
DOIs	https://doi.org/10.1179/175355509X460631
State	Published - 2009
Externally published	Yes

Keywords

Biotemplate
Egg shell
Nanomaterials
PbWO
Synthesis

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10.1179/175355509X460631

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title = "Effect of synthesis conditions on luminescence properties of PbWO 4 nanospheres and nanoflakes",

abstract = "Lead tungstate (PbWO4) nanospheres and nanoflakes have been prepared by template directed synthesis using a biotemplate based on a new egg shell. The product was characterised by X-ray diffraction, scanning electron microscopy and luminescence spectrophotometer. The product morphology could be transformed from nanospheres to nanoflakes via a simple change of solvent. A green emission peak at 480 nm was observed for the flake PbWO4, whereas the emission peak was blue for the PbWO4 nanospheres. The effect of solvent type on the morphology and properties of the synthesised PbWO4 was investigated and a possible formation mechanism for nanospheres or sheets is proposed. The PbWO4 nanocrystals have potential optical applications.",

keywords = "Biotemplate, Egg shell, Nanomaterials, PbWO, Synthesis",

author = "Li, \{M. M.\} and Wu, \{Q. S.\} and Shi, \{J. L.\}",

year = "2009",

doi = "10.1179/175355509X460631",

language = "英语",

volume = "24",

pages = "108--110",

journal = "Materials Technology",

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TY - JOUR

T1 - Effect of synthesis conditions on luminescence properties of PbWO 4 nanospheres and nanoflakes

AU - Li, M. M.

AU - Wu, Q. S.

AU - Shi, J. L.

PY - 2009

Y1 - 2009

N2 - Lead tungstate (PbWO4) nanospheres and nanoflakes have been prepared by template directed synthesis using a biotemplate based on a new egg shell. The product was characterised by X-ray diffraction, scanning electron microscopy and luminescence spectrophotometer. The product morphology could be transformed from nanospheres to nanoflakes via a simple change of solvent. A green emission peak at 480 nm was observed for the flake PbWO4, whereas the emission peak was blue for the PbWO4 nanospheres. The effect of solvent type on the morphology and properties of the synthesised PbWO4 was investigated and a possible formation mechanism for nanospheres or sheets is proposed. The PbWO4 nanocrystals have potential optical applications.

AB - Lead tungstate (PbWO4) nanospheres and nanoflakes have been prepared by template directed synthesis using a biotemplate based on a new egg shell. The product was characterised by X-ray diffraction, scanning electron microscopy and luminescence spectrophotometer. The product morphology could be transformed from nanospheres to nanoflakes via a simple change of solvent. A green emission peak at 480 nm was observed for the flake PbWO4, whereas the emission peak was blue for the PbWO4 nanospheres. The effect of solvent type on the morphology and properties of the synthesised PbWO4 was investigated and a possible formation mechanism for nanospheres or sheets is proposed. The PbWO4 nanocrystals have potential optical applications.

KW - Biotemplate

KW - Egg shell

KW - Nanomaterials

KW - PbWO

KW - Synthesis

UR - https://www.scopus.com/pages/publications/72449186212

U2 - 10.1179/175355509X460631

DO - 10.1179/175355509X460631

M3 - 文章

AN - SCOPUS:72449186212

SN - 1066-7857

VL - 24

SP - 108

EP - 110

JO - Materials Technology

JF - Materials Technology

IS - 2

ER -

Effect of synthesis conditions on luminescence properties of PbWO ₄ nanospheres and nanoflakes

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Keywords

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